Development and optimization of a HS-SPME-GC-MS methodology to quantify volatile carbonyl compounds in Port wines

A method based on headspace solid-phase microextraction (HS-SPME) coupled to gas chromatography-triple quadrupole/mass spectrometry detection (GC-TQ/MS) with a prior derivatization step with O-(2,3,4,5,6-pentafluorobenzyl)hydroxylamine hydrochloride (PFBHA) was developed to quantify carbonyl compoun...

Full description

Bibliographic Details
Main Author: Moreira, Nathalie (author)
Other Authors: Araújo, Ana Margarida (author), Rogerson, Frank (author), Vasconcelos, Isabel (author), Freitas, Victor de (author), Pinho, Paula Guedes de (author)
Format: article
Language:eng
Published: 2018
Subjects:
Port wine
Carbonyl compounds
Quantitative analysis
Derivatization method
PFBHA
Headspace solid-phase microextraction
Gas chromatography-triple quadrupole/mass spectrometry
Central composite design
Online Access:http://hdl.handle.net/10400.14/25691
Country:Portugal
Oai:oai:repositorio.ucp.pt:10400.14/25691

Internet

http://hdl.handle.net/10400.14/25691

Similar Items