A sensitive method for the rapid determination of underivatized ethyl carbamate in fortified wine by liquid chromatography-electrospray tandem mass spectrometry

This work presents the optimization of a miniaturized liquid-liquid extraction (mLLE) followed by reversed-phase liquid chromatography-electrospray tandem mass spectrometry (RP-HPLC-MS/MS) for the determination of ethyl carbamate (EC) in fortified wine, without using derivatizing agents. The mLLE wa...

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Bibliographic Details
Main Author: Leça, João M. (author)
Other Authors: Pereira, Vanda (author), Pereira, Ana C. (author), Marques, José C. (author)
Format: article
Language:eng
Published: 2021
Subjects:
Ethyl carbamate
Liquid-liquid extraction
Wine
Liquid chromatography-mass spectrometry
Design of experiments
.
Faculdade de Ciências da Vida
Faculdade de Ciências Exatas e da Engenharia
Online Access:http://hdl.handle.net/10400.13/3725
Country:Portugal
Oai:oai:digituma.uma.pt:10400.13/3725

Internet

http://hdl.handle.net/10400.13/3725

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