Kinetic modeling of the inverse suspension production of acrylic gels using in line FTIR-ATR monitoring and off-line SEC/RI/MALLS product characterization

This work describes the production of acrylic gels in a batch stirred reactor at 1.5 dm3 scale. Inverse suspension technique is used within this purpose. Paraffin (P) was used in the continuous phase and polymer networks were synthesized in the dispersed phase containing water (W) dissolved acrylic...

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Bibliographic Details
Main Author: Gonçalves, Miguel A.D. (author)
Other Authors: Pinto, Virgínia (author), Dias, Rolando (author), Costa, Mário Rui (author)
Format: conferenceObject
Language:eng
Published: 2010
Subjects:
Acrylic
Gels
In-Line FTIR-ATR
SEC/RI/MALLS
Online Access:http://hdl.handle.net/10198/2580
Country:Portugal
Oai:oai:bibliotecadigital.ipb.pt:10198/2580
Description
Summary:This work describes the production of acrylic gels in a batch stirred reactor at 1.5 dm3 scale. Inverse suspension technique is used within this purpose. Paraffin (P) was used in the continuous phase and polymer networks were synthesized in the dispersed phase containing water (W) dissolved acrylic acid (AA), trimethylolpropane triacrylate (TMPTA), used as crosslinker, and 2,2’-azobis(2-methylpropionamidine) dihydrochloride (V50) as a free radical initiator.

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