Supercritical fluid extraction of Rumex Acetosa L. roots: Yield, composition, kinetics, bioactive evaluation and comparison with conventional techniques

In this study, Rumex Acetosa extracts were obtained from extraction techniques with supercritical fluid (SFE), Soxhlet and low pressure solvent extraction (LPSE). In the SFE, it was evaluated the effect of the process variables (temperature, solventflow rate,pressure andcosolvent concentration) onth...

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Detalhes bibliográficos
Autor principal: Santos, Ênio Rafael de Medeiros (author)
Outros Autores: Oliveira, Humberto Neves Maia de (author), Oliveira, Eduardo de Jesus (author), Azevedo, Saulo Henrique Gomes de (author), Jesus, Anderson Alles de (author), Medeiros, Aldo Miro de (author), Dariva, Claudio (author), Sousa, Elisa Maria Bittencourt Dutra de (author)
Formato: article
Idioma:eng
Publicado em: 2021
Assuntos:
Texto completo:https://doi.org/SANTOS, Ênio R.M.; OLIVEIRA, Humberto N.M.; OLIVEIRA, Eduardo J.; AZEVEDO, Saulo H.G.; JESUS, Anderson A.; MEDEIROS, Aldo M.; DARIVA, Claudio; SOUSA, Elisa M.B.D.. Supercritical fluid extraction of Rumex Acetosa L. roots: yield, composition, kinetics, bioactive evaluation and comparison with conventional techniques. The Journal of Supercritical Fluids, [S.L.], v. 122, p. 1-9, abr. 2017. Disponível em: https://www.sciencedirect.com/science/article/abs/pii/S0896844616303734?via%3Dihub. Acesso em: 20 abr. 2021. https://doi.org/10.1016/j.supflu.2016.11.019
https://doi.org/10.1016/j.supflu.2016.11.019
País:Brasil
Oai:oai:https://repositorio.ufrn.br:123456789/32680
Descrição
Resumo:In this study, Rumex Acetosa extracts were obtained from extraction techniques with supercritical fluid (SFE), Soxhlet and low pressure solvent extraction (LPSE). In the SFE, it was evaluated the effect of the process variables (temperature, solventflow rate,pressure andcosolvent concentration) onthe extraction kinetics, yield and extract solubility. In the Soxhlet extraction, it was evaluated the usage of ethanol, acetonitrile, isopropanol and tert-butyl alcohol, while in LPSE extraction, it was used ethanol as solvent. The phenolics total content (TPC), antioxidant capacity (IC50) and extract composition were determined. The yield obtained ranged from 0.2 to 8.3%. The SFE extraction has demonstrated great efficiency in the extraction of phenolic compounds (anthraquinone and stilbene). The trans-resveratrol concentration in the extracts ranged between 1.03 and 3.52 mg/g, depending on the technique used, the values of IC50 and TPC ranges from 10.67 to 163.43 g/mL and 27.63 to 157.04 mgEAG/g, respectively